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NHTNO'lS'` ُ{|ߘT(Wؚ)nؚS NReQkxxTؚ/lxMbmS[hQ[9]0[N+TlbRؚvߘT7hT Y iirl0CheI{ (WReQmTxT 1uN7hTnm(Wmxhb N [fb_b[tev Rpemb N ggRpvS^ [f brlbޘn Vdk ^7hTy7hϑ NؚN1 g iirlg}Y:N0.1~0.2 g Te(WmǏ z-NeeR]xx 8^SReQ]xxؚ/lxmTm15 mL >enǏYvQba'lS !kemSǏ z-N؏eRmTx10 mL]S0R{|7hTYaR0gR VvQ+T g'YϑvYN (WRmTxmSKNMRN[RpScYNla Nr^m _YN%cS[kT QReQxmS0 [Nm`ߘT-Nv gkCQ }Rg ؏SNǑ(uzʑlT4ltmr^l0Km[ߘeSvczʑTRgKm[ }vRI{R{|vKm[RǑ(u.llR4ltmr^lvHeg}Y[10]0 13.3 ߘTRg^(u[O 13.3.1 7{|0{|0m|SvQ6RTRg 13.3.1.1 ICP-AESKm[ߘT-NŔ07x000 0ݔ00A0|x000ܔ00060!0I00[11] t$ elc Ջ7h~ǏmT 7hmvc[eQ5ua&TI{yP[SOSP[S\IQ1NKm[ hQf~l[ϑ0 u$ NhVNՋBR 5ua&TI{yP[SOSP[S\IQ1N0 Km[CQ }hQPYm cGB/T 602vĉ[M6Rb1uV[hQir(xvz-N_cO v^9hncM6RbTCQ }hQ|RO(um0 ]xx Ǐ'lS"l ؚ/lx ]xx kxS "l'lS @b(uՋBRGW:NO~~0)ll~^e"99.99% 0[(u4l^&{TGB/T 6682-NN~4lvĉ[0 v$ Rgek 7hT6RYS (ur^ppSl0nmlT_lml Nyel-NvNNymՋ7h0 r^ppSl7xdY yS5~10 g|7{|5~10 g4lg0,܃{|02~5 g6RT 1~5 g4lNT Ջ7hNtiWW-N HQ(W5up N\kppSep 6qTyeQؚ)np-N N500!ppS6~8 h0Ջ7hppS N{_^ RS(W7hTSQQtSTnRpen]xx (W5up Nr^T͑enNؚ)np-NppS v7hTSbpp}vr:Nbk SQ>eQ0(u\ϑ5%]xx\ppRn v^\mSmmeQbneQ10~15 mL[ϑt-N[[mS0 nlmyS2~5 g|7{|2~5 g4lg0,܃{|01~3 g6RT 1~2 g4lNT Ջ7hϑՋ7hN100 mL N҉t-N ReQ20 ~30 mL]xxxmlǏY0tSRN\oenN5upg NRpm0傈m㉲mSm)10 mL]SN g*gRirbrm S N>eQ eR]xx5~10 mL vmSmHTerfbeu&^Ğr0ReQ1~2 mLmx]xx+ؚ/lx  EMBED Equation.DSMT4 =4:1 SQ}vp S N>eQ eR\ϑ0.5 mol/L]xx (u\ϑ4lQmtX (W5upg NRpNdSǏϑv]xx S N>eQ0\m㉲myeQ10~50 mL[ϑt-N[[mS0 _lmyS0.5~2g|7{|0.5~2 g4lg0,܃{|00.5 g6RTT4lNT Ջ7hNZVlYNpmP-N R5~10 mL]xxxmlǏY QR1~3 mLǏ'lS"l v}Y[hQT \mP>eeQ_lpm|~0n z^vm㉌[hQ0S\mP>e(W5upg NRpNdSǏϑv]xx S N>eQ0\m㉲myeQ10~50 mL[ϑt-N[[mS0 Km[agNؚSuhVRs1100 w0QtSlAmϑ20 L/min RlAmϑ0.3 L/min SlAmSR0.24 MPa0Rlۏ7hϑ 1.0 mL/min0Km[ߘT-NTCQ }vRg~lThQPRNh13-10 h13-1Km[TCQ }vRg~lTelhQP Rg~l/nmhQP/g" mL-1Rg~l/nmhQP/g" mL-1Pb 220.3530.03Mn 257.6100.015As 193.7590.03Cu 324.7540.003Fe 259.9400.03Ba 455.4030.003Ca 319.9330.3Ti 336.1220.03Zn 213.8560.15Sr 407.7710.003Al 308.2150.15Sn 235.4840.15Na 589.5920.3Cd 226.5020.03Mg 279.5530.03Cr 267.7160.3B 249.7720.015V 292.4010.3w$ elċN elvhQPh13-10(uN7ir0m|06S0|p0,܃04lgSvQ6RT0NS4lNT0\uy0ne0qL܃0sTTI{ߘTRg0 x$ laNy `$ [NqL܃0sTTI{ؚv+Tϑ7hT SNǑ(uqQlml[ƖKmCQ }0Ջ7hYte\m㉲mhQlypog-N ReQ3 mg/mL]xx1 mL ReQ50%"l'lS(ux^QnxpH 10 ReQ2.4 mg/mLkxS2~3 mL mS Yn1~3 h0leQy_{ v^(u\ϑY!kmmpog mmTv^Ny_{-N (W~5000 r/min Ny_10~20 min0_Sy_{-N NB\nm OYulm0QReQϑ4l GdS Q!ky_ S Y2!k0gT(u5 mLv0.5 mol/L]xx\lmnv^leQ10~50 mL[ϑt-N[[0 a$ [-NmSvSRmP0[ϑtTym{I{(WO(uMR(u10%v]xxnm-NxmlǏY 6qT(uN!k4lbSyP[4lQmr^Q0 13.3.1.2 ICP-AESKm['Ys||0\|-Nvݔ000ܔ00A000060 0[12] t$ elc (uSm]xx0vxTؚ/lxRpmՋ7h m㉲mvc[eQ5ua&TI{yP[SOSP[S\IQ1 TeKm[11yё^\CQ }0 u$ NhVNՋBR Optima 2100DVW5ua&TI{yP[SOSP[S\IQ1NVPerkin-ElmerlQS 0 ]xx ؚ/lx vxI{@b(uՋBRGW:NO~~0[(u4l:NwNl4l0 1000g/mLvZn0Fe0Mn0Ca0Mg0RbT MoUSCQ }hQPYnmGW:NV[hQnm0100g/mL Sr0Cu0Ba0AlvmThQPYnm(GSB 04-1767-2004)0 HNO3,HClO4,HCl GW:NO~~0[(u4l:NwNl4l0 v$ Rgek yS1.000g0.010 gr^qՋ7hnN%b_t-N R+RReQ8 mL Sm]xx 2 mLؚ/lxT1 mLSmvx nN5upg N (W150!]SRpĞpQ=\ Sm)m㉲m~1~2 mL S Nv^QtS06qTReQ8 mL Sm]xx Yn (W5upg NQRp5 min]S S NYnQtS (u4lly50 mL[ϑt-N[[0 Km[agNؚSuhVRs1300W0QtSlAmϑ15 L/min RlAmϑ0.5 L/min SlAmϑ0.8 L/min0Ջ7hۏ7hϑ1.5 mL/min tTI{yP[SO‰Km0 w$ RgċN Km[TCQ }vRglh0hQP0~'`R`VTRghQir(v~gRNh13-20RghQir(\|NIST8436 Qnx^(W98.24~138.74KN RSDn=6 :N1.76~13.950 h13-2 Km[TCQ }vRg~l0~'`R`V0hQPNQnx^ Rg~l/nm~'`V/mg" L-11hQP/mg" L-1hQSir(h:yeQ|sts ReQ10~20 mLmx]xx+ؚ/lx  EMBED Equation.DSMT4 =4+1 m RvN\oebhbv xmlǏY !ke(W5upg NRpm}vpQs Nm㉲mHTerfbeu>fĞr:Nbk0QtSTly25 mL[ϑt-N[[0 _lmySՋ7h0.5~1 gnNZVlYNpQP-N ReQ5 mLSm]xx xml30 min QReQ2 mL 30%Ǐ'lS"l >en5 min v NQv [ňObWY >eeQ_lm|~ n z^mՋ7h0m~_gTSQQP lym㉲mN10 mL[ϑt-N[[0 r^ppSlyS1~5 gՋ7hnNiWW-N HQ\kp(W5upg NpSep QnN550 !vؚ)n5u;p-NppS4~5 he QtS0ppS N{_^ SQ>eQRQn]xxmn (W5upg Nr^qT͑eppS0SQppS}YvՋ7hReQ10 mLv0.5 mol/L]xxnm >e(W5upg NNO)nRpnppR ly25 mL[ϑt-N[[0 Km[agNNhVd\OvSagNRN13-30Km[CQ }e ^ReQ50g/Lgnm O_Kmnm-Ngvg~Sm^:N5 g/L0 h13-3 Km[7irSvQ6RT-Nܔ0000 00A Rg~l/nm IQ1&^/nmhQP/mg" kg-1~'`R`V/mg" L-1 Cu 324. 80.70.60.1~1.0 Fe 248. 30.22.40.5~4.0Mn 279. 50.20.50.5~4.0Zn 213. 90.70.40.2~1.5Ca 422. 70.71.50.5~5.0Mg 285. 20.20.70.2~2.0w$ elċN elvhQPT~'`R`VRNh13-30(W͑ Y'`agN N $N!ks^LKm[~gv~[]

eBRLa3 + 0Sr2 + SNmd0X[(W5uyr^pb ReQxё^\vSNmd0 ݔ0x0I{CQ }[0 gSf[r^pb ReQʑ>eBRxW4lhgxSNmd0 13.3.1.6 JmpS-kp0qSP[8T6eIQ1lKm[ߘT-NvI[16] t$ elc Ջ7h[hQmT ReQKIOvQ-NvCd2-NI-S^ubCdI42- 6qTN2uW~MG u4lyP[Tb_b YTir0Triton X-114S bxmT zʑTvSm^V (uzzl-YNpkp0qSP[8T6eIQ1lKm[I0 u$ NhVNՋBR TAS-986WSP[8T6eIQ1NSNnfgNhVlQS 0 /lSI 2.0 mol/L KI 1.5mmol/L2uW~ Triton X-114 (4.5%) YNxpH 4.0 vxT"l'lS @b(uՋBR:NRg~0hQnmPX[(WZYNp[hV 4!OX[0 v$ Rgek 7hT6RYyS0.5000 gv'Ys|0+}܃0wm&^NmP-N ReQ1.0 mLSm]xxT3.0 mL 30%Ǐ'lS"l ^e_>enǏY06qT[\nN_lmN-Nm (W100!Rp1 h 140!Rp3 h m㉌[kT>eQ0SQmP (WRpg NSr^ kYuir(u5%]xxn ly25 mL[ϑt-Nzʑ0R;R^0 JmpSyS9.00 mLՋ7hbhQir(m㉲mN15 mLy_{-N ReQ2.0 mL 2.0 mol/L KInm 2.0 mL1.50 mmol/L MGnmT1.0 mL 4.5%Triton X-114nm0(uYNxx^:NpH 5.0 (u4l[[;R^0\y_{nN50!4ltmR`)n15 minTSQ (W3800 rpml Ny_10 min O4lvN[+Thb;m'`BRv g:gvRy0[Ɩ|pe:N13.50QtmQtSO g:gvSϞ z (ul\hV[hQ8TQ Nnm0T g:gv-NReQ+T]xxv2unm0.6 mL GdST[eQSP[8T6eIQ1NKm[0 Km[agNRg~lCd 228.8nm0IQ1&^ 0.4nm zz_4gop5uAm 2.0mA0qphVؚ^ 6.0mm qlAmϑ 1500 mL/min0 w$ elċN lhQP(3):N0.9 ng/mL [ϑP(10):N3.0 ng/mL0RSDc=50 ng mL-1, n=7 :N4.2%0V6es:N90.0%~110%0~'`R`V2.0~200 ng/mL Rg'Ys||V[hQir(GBW 08510 Km[

eQT b~gQScl Q\mPb_0\m㉶nmyeQ25 mL[ϑt-N R2 mLvnm R4lzʑ;R^0 bySGWSՋ7h0.5 g~1.0 gnN150 mL%b_t R15 mL~20 mL]xx vhbv>enǏY0nN5upg NRpяr^0>eQTR2 mL~4 mLǏ'lS"l QRpяr^0>eQ \7hmyy0R25 mL[ϑt-N R2 mLvnm R4lzʑ;R^0 Km[agNRg~l Ge 265.2 nm0IQ1&^0.4 nm zz_4gop5uAm10 mA0pwX{ wXpvGS)n z^/f80!~120!r^q30s Q(W120!~300!r^q20s300!ppS30s 1200!SP[S20s 2700!QS3s0hQf~l[ϑ0 w$ elċN elhQP:N40pg !hckf~~'`R`V NP:N200 ng/mL0el(uN7ir0F{|0,܃Tˆ{|-NvKm[0 13.3.1.8 wXpSP[8T6eIQ1lKm[;z7-NvuϑŔ0I[18] t$ elc Ջ7hǏnml[hQmS 6qT[eQwXpSP[8T6eIQ1NKm[0 u$ NhVNՋBR SP[8T6eIQ1N0 hQPYnm-V[hQ-N_0 ]xx Ǐ'lS"l kxx vx ؚ/lxGW:NO~~0[(u4l:NN~4l0[MR^[4lTՋBRۏLalgՋ0 v$ Rgek 7hT6RY7hT~R7hT SdBg((;z71X) ~|xTEQRmS0yS2 gՋ7hKm[Ŕ ReQ15~20 mLmx]xx+ؚ/lx  EMBED Equation.DSMT4 =4+1 0byS1gՋ7hKm[I ReQ10 mLmx]xx+ؚ/lx  EMBED Equation.DSMT4 =4+1 xmlǏY06qT>e(WRpg NRpmS HQbaRpeĞpNu 6qTcؚ)n^ S_nmQs}vpS^_Yope S_MNO)n^2bkm㉶nmUnTpS0傶nmrm eR1~2 mLmxnmrSehĞr QtS ly25 mL[ϑt[[0 Km[agN[vwXpvRp z^RNh13-60lopb^XfHe^!hck̀of0hQf~l[ϑ0 h13-6Km[;z7-NvuϑŔ0IvRp z^ Km[ŔvRp z^Km[IvRp z^)n^/!e/s)n^/!e/sr^q80~1201580~12015r^q1201512015ppS450~55015450~55015ppS650~6501555015SP[S2100519005QS2300321003 w$ elċN Km[ŔTIvhQPR+R:N0.005 g/kgT 0.1 g/kg Ǒ(uꁨRۏ7h RSDd"5Ǒ(uKbRۏ7h NOSm^:SRSDd"25 ؚSm^:SRSDd"100 RghQir('Ys|| Ŕvh:yeeQ( EMBED Equation.DSMT4 =10%) HClnmxmlǏY0 a$ HQ(uHNO3 ( EMBED Equation.DSMT4 =10%)nmxmlnm15 ~30 min 6qT>eeQ( EMBED Equation.DSMT4 =10%) HClnmxmlǏY0 b$ HQ(u( EMBED Equation.DSMT4 =10%) HNO3nmxmlnm15 ~30 min 6qTLpnؚ0xnmxmlǏY0 13.3.1.10 "lSirSu-SP[gIQIQ1l[|ߘ-NRx+TϑvKm[[20] t$ elc Ǒ(uޏ~AmR(ۏ7h)"lSirSu-SP[gIQIQ1l (uϑv0lS\Or^pbb6RBRbR0WmdNCu0BiI{CQ }vNpb _0upOe0QnxKm[|ߘ-N_ϑRx0 u$ NhVNՋBR AF-610ASP[gIQIQ1N(SN^t)RRgNhVlQS)0 1.0 mg/mlRxhQPYnmM6RelS,gfNDU_30 10g/L|x"lSnm0]xx0ؚ/lxGW:NO~Rg~0[(u4l:NN!k4l0 v$ Rgek 7hT6RYyS2.OOOg(Qnx0.1mg)Θr^|xǏ40v[{v|ߘ7hTnN250mL%b_t-N ReQ10mL]xx-ؚ/lxmTnm (WtSYnN/_\oe QmSǏY !kenN5up NRpmS Yxm\SϑeR RpmSQ}vp ~~Rp\SOy(~2mL R NSr^)0S NQtST ReQ5mLvxnm QnN5up NRp g}vpQQ nmnNer S NQtSTly0RHQR g1.5mL10g/L0lSnmv25mL[ϑt-N (u4l[[0 Km[agNIQ5u PX{ؚS300V0zz_4gop5uAm70~80mA0SP[ShVp)n^NO)n SP[ShVpؚ^7mm0}lAmϑ800mL/min0pee12s ^ߏe3s ۏ7he16s Ǒ7he5s0 w$ elċN elhQP:N0.34ug/L, v[hQOP]n=7 :N3.80V6es93.2^1020~'`R`V NP250ug/L0 x$ laNy (W10lSX[(WagN N 1000 PvAs0Pb0Mn0Te 500 PvSn0Hg 100 PvCu0Bi Nr^pb|ߘ7hT-NRxvKm[0 13.3.2 F{|SvQ6RTRg 13.3.2.1 ICP-AES lKm[F{|ߘT-Nv_ϑCQ }[21] t$ elc Ǒ(uؚS]xSPm7hT NICP-AESlKm[TF{|ߘT-NCa Mg Mn Sr Fe Co Ni Se Ba I{YyuϑCQ }v+Tϑ0 u$ NhVNՋBR DREW5ua&TI{yP[SP[S\IQ1NV)RfLeemanlQS 0 1000ug/mL Ca Mg Mn Sr Fe CO Ni Se BahQPYnm(Qё萢xvz;`bV[PgeKmՋ-N_),mThQnm(u2%]xx~zʑhQPYnmM6R0 ]xx ؚ/lxGW:NO~~0 v$ Rgek 7hT6RYyS0.5g]SĞF0~F0ўF0~F7hT (W5up NxSep (Wl_p-NN600!ppS1h0SQT zQ>eeQؚS]xSP-N ReQ5mL]xx02mLؚ/lx02mL"llx b'} Nv 130!R`)n{>en4h0SQ zQT yeQ50mL[ϑt-N ReQ2nS'l4l 0.5mL]xx v^NSyP[4l[[0S5mLՋmzʑ5 P (uICP-AES Km[0 Km[agNRg~lBa 455.403 nm0Co 228.162 nm Mn 257.610 nm Sr 407.771 nm Ni 221.647 nm Se 196.026 nm Fe 238.204 nm Ca 393.336 nm Mg 279.553 nm0I{yP[SORs1.0 KW0)llSR0.6 MPa0QtSlAmϑ15 L/min RlAmϑ0.2 L/min ShVSR374.06 Pa07hmcGSϑ1.5 mL/min0‰[MOnꁨROS0 w$ elċN 9yCQ }vhQP:N0.0003~0.004 ug/g RSDn=5 :N0.07%~3.35% RhV6es:N96.8%~102%0 13.3.2.2 wXpSP[8T6eIQ1lKm[ߘT-NvŔ[22] t$ elc Ջ7h~ppSbxmT leQSP[8T6eIQ1NvwXp-NKm[ hQf~l[ϑ0 u$ NhVNՋBR SP[8T6eIQ1NDwXpSŔzz_4gI{ 0 @b(uՋBR]xx Ǐkxx Ǐ'lS"l ؚ/lx xxN"lI{GW:NO~~0 v$ Rgek 7hT6RYF{|T|ߘdSBgirTxx Ǐ20v[{0[N4lR+Tϑؚv,܃04lg0|{|0{|Tˆ{|T ^HQSFmQyϑ0Ջ7hmSǑ(uSRmPml0r^ppSl0ǏkxxppSlbnmlVyel0 SRmyS 1 g~2 gՋ7h[N+TؚvF{|Ջ7h1 g NZVlYNpQP R2~4 mLSm]xxxmlǏY0QR2~3 mL 30%Ǐ'lS"l;`ϑ NǏP[yv 1/3 0v}Y e'} >eeQR`)nr^q{ 120~140 !Oc 3~4 h QtSTSQ ƉmSTՋ7hvvR+Tϑ\mSm[hQleQ10 mLb25 mL [ϑt-N[[0 r^ppSlyS 1~5 g Ջ7hNtiWW-N HQ\kp(WS_5upg NpSep yeQl_pN500 !25 !ppS 6~8 h QtS0*N+RՋ7hppS N{_^ RReQ1 mL]xx+ؚ/lx9+1 (WS_5up N\kpRp S YY!kv0RmS[hQ0>eQ (u0.5 mol/L]xxnppR [hQleQ[ϑt-N[[0 ǏkxxppSlyS 1~5 g Ջ7hNtiWW-N R 2~4 mLSm]xxxml 1 h N N HQ\kppS QtSTR 2.00~3.00 g ǏkxxvN Nb ~~pS NQp leQl_p 500!25!R`)n 2 h, QGS 800! Oc 20 min0QtS R 2~3 mL 1mol/L]xx \mSmleQ[ϑt[[0 nmlySՋ7h 1 g~5 g|nx0R 0.001 g N%b_tbؚpog-N >epe|sts R10 mLmx]xx+ؚ/lx, EMBED Equation.DSMT4 = 9+1 RvxmlǏY RN\oeN5up Nm Shўr QRmTx vQ}vp mSmHTerfbeu&^Ğr0>eQ \mSmleQ[ϑt[[0 Km[agNRg~lPb 283.3 nm0IQ1&^0.2~1.0 nm zz_4gop5uAm5~7 mA r^q)n^120! 20sppS)n^ 450! Oc15 ~20 s SP[S)n^1700~2300! Oc4~5s0lopb^XfHe^!hck̀of0hQf~l[ϑ0 w$ elċN elhQP:N 0.005 mg/kg0 x$ laNy `$ gWSOr^pb RleQϑN,:N5 L Sf[9eۏBR20g/LxxN"lnm mdWSOr^pb0 a$ |[^Bl(W͑ Y'`agN N_v$N!krzKm[~gv~[]

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